Apparatus and method for gas chromatography

G - Physics – 01 – N

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G01N 30/88 (2006.01) G01N 27/62 (2006.01) G01N 30/68 (2006.01)

Patent

CA 2261860

The apparatus (10) comprises an injector (11) for products to be analysed, a column for splitting (12) said products, a detector (13) of the flame ionisation detector type and a device (14) for producing fuel gas. This device (14) comprises an electrolyzer outfit (15) containing distilled water or an aqueous solution of caustic soda (NaOH) or caustic potassium (KOH), in which are immersed two electrodes (16, 17). These electrodes are supplied by an electric energy source (18). Hydrogen and oxygen are formed at the electrodes and are transmitted, without separation, by means (19) for supplying said flame ionisation detector with hydrogen and oxygen.

L'appareil (10) comporte un injecteur (11) pour des produits à analyser, une colonne de séparation (12) desdits produits, un détecteur (13) du type détecteur à ionisation de flamme et un dispositif (14) de production de gaz de combustion. Ce dispositif (14) comporte un dispositif d'électrolyse (15) contenant de l'eau distillée ou une solution aqueuse de soude caustique (NaOH) ou de potasse caustique (KOH), dans laquelle plongent deux électrodes (16, 17). Ces électrodes sont alimentées par une source d'énergie électrique (18). De l'hydrogène et de l'oxygène se forment aux électrodes et sont transmis, sans séparation, par des moyens (19) pour alimenter ledit détecteur à ionisation de flamme en hydrogène et en oxygène.

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