Polymeric compositions for soil release on fabrics

C - Chemistry – Metallurgy – 08 – F

Patent

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C08F 220/24 (2006.01) C08F 220/34 (2006.01) C08L 33/14 (2006.01) C08L 33/16 (2006.01) D06M 15/263 (2006.01) D06M 15/267 (2006.01) D06M 15/273 (2006.01) D06M 15/277 (2006.01)

Patent

CA 2330051

A copolymer composition and its use as a soil release agent for fabrics comprising monomers copolymerized in the following percentages by weight: (a) from about 30 % to about 49 % of at least one monomer of formula (I): Rf-Q-A- C(O)-C(R)=CH2, wherein Rf is a straight or branched-chain perfluoroalkyl group of from 2 to about 20 carbon atoms, R is H or CH3, A is O, S or N(R'), wherein R' is H or an alkyl from 1 to about 4 carbon atoms, Q is alkylene of 1 to about 15 carbon atoms, hydroxyalkylene of 3 to about 15 carbon atoms, - (CnH2n)(OCqH2q)m-, -SO2-NR'(CnH2n)-, or -CONR'(CnH2n)-, wherein R' is H or an alkyl of from 1 to about 4 carbon atoms, n is 1 to about 15, q is 2 to about 4, and m is 1 to about 15; (b) from about 10 % to about 70 % of at least one monomer or a mixture of monomers selected from the formulae (IIA): (R1)2N- (CH2)r-Z-C(O)-C(R2)=CH2, (IIB): (O)(R3)(R4)N-(CH2)r-Z-C(O)-C(R2)=CH2, (IIC): X- (R5)(R4)(R3)N+-(CH2)r-Z-C(O)-C(R2)=CH2, wherein Z is -O- or -NR5-; R1 is an alkyl group of from 1 to about 3 carbon atoms; R2 is H or an alkyl radical of 1 to about 4 carbon atoms; R3 and R4 are each an alkyl of 1 to 4 carbon atoms, hydroxyethyl, benzyl, or R3 and R4 together with the nitrogen atom form a morpholine, pyrrolidine, or piperadine ring; R5 is H or an alkyl of 1 to 4 carbon atoms, or R3, R4 and R5 together with the nitrogen atom form a pyridine ring; r is 2 to 4; and wherein for formula (IIA) the nitrogen is from about 40 % to 100 % salinized; and (c) eventually other monomers.

L'invention concerne une composition de copolymères et son utilisation comme agent antisalissures pour tissus. La composition comprend des monomères copolymérisés selon les pourcentages en poids suivants: a) 30 à 49 % environ d'au moins un monomère de formule (I): R¿f?-Q-A-C(O)-C(R)=CH¿2?, dans laquelle R¿f? est un groupe perfluoroalkyle à chaîne droite ou ramifiée renfermant 2 à environ 20 atomes de carbone; R est H ou CH¿3?; A est O, S ou N(R'), où R' est H ou un alkyle renfermant 1 à environ 4 atomes de carbone; Q est alkylène renfermant 1 à environ 15 atomes de carbone, hydroxyalkylène renfermant 3 à environ 15 atomes de carbone, -(C¿n?H¿2n?)(OC¿q?H¿2q?)¿m?-, -SO¿2?-NR'(C¿n?H¿2n?)-, ou -CONR'(C¿n?H¿2n?)-, où R' est H ou un alkyle renfermant 1 à environ 4 atomes de carbone, n est compris entre 1 et environ 15, q est compris entre 2 et environ 4, et m est compris entre 1 et environ 15; b) 10 à 70 % environ d'au moins un monomère ou un mélange de monomères choisis entre les formules (IIA): (R¿1?)¿2?N-(CH¿2?)¿r?-Z-C(O)-C(R¿2?)=CH¿2?, (IIB): (O)(R¿3?)(R¿4?)N-(CH¿2?)¿r?-Z-C(O)-C(R¿2?)=CH¿2?, (IIC): X?-¿(R¿5?)(R¿4?)(R¿3?)N?+¿-(CH¿2?)¿r?-Z-C(O)-C(R¿2?)=CH¿2?, dans lesquelles Z est -O- ou -NR¿5?-; R¿1? est un groupe alkyle renfermant 1 à environ 3 atomes de carbone; R¿2? est H ou un radical alkyle renfermant 1 à environ 4 atomes de carbone; R¿3? et R¿4? sont chacun alkyle renfermant 1 à 4 atomes de carbone, hydroxyéthyle, benzyle, ou bien R¿3? et R¿4? forment avec l'atome d'azote un noyau morpholine, pyrrolidine ou pipéradine; R¿5? est H ou un alkyle renfermant 1 à 4 atomes de carbone, ou bien R¿3?, R¿4? et R¿5? forment avec l'atome d'azote un noyau pyridine; r est compris entre 2 et 4; et pour la formule (IIA), l'azote est salinisé à un pourcentage compris entre environ 40 % et 100 %; et c) éventuellement d'autres monomères.

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