Industrial process for preparing diethyl...

Details Industrial process for preparing diethyl... Industrial process for preparing diethyl...

C - Chemistry, Metallurgy

07

F

260/237.3

C07F 9/60 (2006.01) C07F 9/6561 (2006.01)

Patent

CA 2038976

Synthèse industrielle du N-(desacétyl-0-4 vinblastinoyl-23) amino-1 méthyl-2 propylphosphonate de diéthyle (1S) et de ses sels par condensation de l'acide desacétyl-0-4 vinblastinoïque (obtenu par hydrolyse alcaline du sulfate de vinblastine) sur la phosamine (+) (isomère dextrogyre de l'amino-1 méthyl-2 phosphonate de diéthyle), au moyen du BOP, réactif de couplage peptidique, [hexafluorophosphonate de benzotriazolyl-1 oxy-tris (diméthylamino) phosphonium] ; et si on le désire, le produit obtenu est salifié avec des acides appropriés.

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