Method for synthesis of rhizoferrin

Details Method for synthesis of rhizoferrin Method for synthesis of rhizoferrin

C - Chemistry, Metallurgy

07

C

C07C 229/24 (2006.01) C07C 229/26 (2006.01) C07C 231/02 (2006.01) C07C 235/10 (2006.01)

Patent

CA 2276598

A method of synthesizing rhizoferrin and analogues thereof comprising acylating a protected polyamine with a citric acid diester; hydrolyzing the resulting amide to produce an N-protected rhizoferrin or analogue thereof; and deprotecting the intermediate to produce rhizoferrin or the analogue thereof.

Ce procédé de synthèse de la rhizoferrine et d'analogues de celle-ci comprend les étapes consistant à acyler une polyamine protégée, au moyen d'un diester d'acide citrique, puis à hydrolyser l'amide résultant afin d'obtenir une rhizoferrine N-protégée ou un analogue de celle-ci, et enfin à déprotéger celle-ci ou son analogue, afin d'obtenir une rhizoferrine ou son analogue.

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