Method for producing nitroguanidine derivatives

C - Chemistry – Metallurgy – 07 – D

Patent

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Details

C07D 213/61 (2006.01) C07D 213/89 (2006.01) C07D 277/28 (2006.01) C07D 307/14 (2006.01) C07D 403/06 (2006.01)

Patent

CA 2293681

The invention relates to a method for producing compounds of formula (I), wherein R1 = hydrogen or C1-C4-alkyl; R2 = hydrogen, C1-C6-alkyl, C3-C6- cycloalkyl or a CH2-B radical; A = an unsubstituted or mono or penta- substituted aromatic or non-aromatic monocyclic or bicyclic or heterocyclic radical and B = phenyl, 3-pyridyl or thiazolyl which are optionally substituted by one to three substituents, by hydrolyzing a compound of formula (II), wherein R1, R2 and A have the same meaning as in formula (I) and R3 stands for an unsubstituted or substituted C1-C10-alkyl, C3-C6-cycloalkyl, phenyl or benzyl. The invention is characterized in that the reaction is carried out at a pH value ranging from 7 to 14. The invention further relates to starting materials to implement said method. The compounds of formula (I) are suitable as intermediate products for the production of pesticide mixtures.

L'invention concerne un procédé de préparation de composés de la formule (I) dans laquelle R¿1? désigne hydrogène ou alkyle C¿1?-C¿4?; R¿2? désigne hydrogène, alkyle C¿1?-C¿4?, cycloalkyle C¿3?-C¿6? ou un reste -CH¿2?B; A désigne un reste hétérocyclique monocyclique ou bicyclique, aromatique ou non aromatique, non substitué ou substitué entre une et cinq fois; et B désigne phényle, 3-pyridyle ou thiazolyle, qui sont éventuellement substitués par un à trois substituants; par hydrolyse d'un composé de la formule (II), dans laquelle R¿1?, R¿2? et A ont la signification mentionnée dans la formule (I) et R¿3? désigne alkyle C¿1?-C¿10? non substitué ou substitué, cycloalkyle C¿3?-C¿6?, phényle ou benzyle. Ce procédé se caractérise en ce que la réaction est effectuée à un pH compris entre 7 et 14. L'invention concerne également des produits de départ nécessaires pour mettre ledit procédé en oeuvre. Les composés de la formule (I) s'utilisent comme produits intermédiaires pour préparer des mélanges pesticides.

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