Platinum catalyst composition, method for its preparation...

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400/5313, 252/91

B01J 31/22 (2006.01) B01J 31/16 (2006.01) C07F 15/00 (2006.01) C08G 77/398 (2006.01) C08L 83/04 (2006.01) C08L 83/05 (2006.01)

Patent

CA 2023988

A platinum catalyst composition having improved thermal stability, and all of the utilities of platinum catalyst compositions of the art, is provided by mixing certain organosiloxanes which contain aryl and alkenyl groups, such as 1,3-divinyl-1,3-diphenyldimethyl- disiloxane, in a quantity of at least 2 moles, with a platinum complex having as a ligand an organosiloxane which contains alkyl and alkenyl groups, such as 1,3-divinyltetramethyldisiloxane (or a mixture of said platinum complex and said organosiloxane), in a quantity of 1 mole of platinum atoms. In a preferred embodiment the mixture is distilled in vacuo to remove part or all of the organosiloxane which contains alkyl and alkenyl groups, and most preferably to remove at least a portion of the complexed organosiloxane which contains alkyl and alkenyl groups.

Une composition catalytique à base de platine, à la stabilité thermique accrue, dotée de toutes les fonctions des compositions catalytiques de ce type, est fournie par le mélange de certains organosiloxanes contenant des groupements aryl- et alkényl-, comme le 1,3-divinyl-1,3-diphényldiméthyl-disiloxane, en quantité égale à au moins deux moles, à un complexe du platine comportant comme ligande un organosiloxane qui contient des groupements alkyl- et alkényl-, tel que le 1,3-divinyltétraméthyldisiloxane (ou un mélange du complexe du platine et de l'organosiloxane), en quantité égale à 1 mole d'atomes de platine. Dans une forme préférée, le mélange est distillé sous vide pour éliminer en tout ou partie l'organosiloxane qui contient les groupements alkyl- et alkényl-, et de façon préférentielle, pour supprimer au moins une partie de l'organosiloxane complexé qui contient les groupements alkyl- et alkényl-.

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