Use of a second stage reactor in the manufacture and...

C - Chemistry – Metallurgy – 07 – C

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C07C 43/04 (2006.01) C07C 41/01 (2006.01) C07C 41/09 (2006.01)

Patent

CA 2183490

MTBE is prepared from TBA and MeOH by passing a feed mixture comprising TBA and MeOH through a primary MTBE reaction zone to form a primary reaction product containing MTBE, unreacted TBA, unreacted MeOH, isobutylene and water; the primary reaction product is fractionated to provide a first lighter distillation fraction comprising isobutylene, MeOH and MTBE and a first higher boiling distillation fraction comprising MeOH, TBA and water and the first higher boiling distillation fraction is charged to a second stage MTBE reaction zone to form a second stage reaction product compris- ing unreacted MeOH, unreacted TBA water, isobutylene and MTBE.

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