Method for the preparation of carbon moldings and activated...

C - Chemistry – Metallurgy – 01 – B

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C01B 31/08 (2006.01) C01B 31/00 (2006.01) C01B 31/02 (2006.01) C01B 31/14 (2006.01) C04B 35/52 (2006.01) C10C 3/00 (2006.01) D01F 9/145 (2006.01)

Patent

CA 1036771

ABSTRACT OF THE DISCLOSURE A method for the preparation of a porous carbon molding having a low apparent density, the method comprising the steps of thermally mixing a pitch, which has a softening point of 50-350°C, a carbon content of 80-97 wt%, a hydrogen/ carbon ratio of 0.3-2.5 and a nitrobenzene-insoluble fraction of below 60 wt%, with at least one aromatic hydrocarbon having a boiling point of 200°C or higher, forming the mixture into a suitable shape, immersing the formed material in a solvent, in which the pitch is hardly soluble but the aromatic hydrocarbon is easily soluble, for extracting the aromatic hydrocarbon from the formed material and obtaining a porous pitch material, oxidizing the porous pitch material at a temperature from room temperature to 400°C by the use of an oxidizing agent to form an infusible porous pitch material, and calcining the infusible porous material in an inert atmosphere at a temper- ature higher than 600°C to obtain a porous carbon material. The porous carbon material or the infusible porous material may be activated by means of steam vapour or air to produce an activated carbon material.

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