Cryostat for superconducting nmr spectrometer

F - Mech Eng,Light,Heat,Weapons – 17 – C

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F17C 1/00 (2006.01) G01R 33/31 (2006.01) G01R 33/3815 (2006.01)

Patent

CA 1104054

PATENT APPLICATION of GEORGE D. KNEIP, JR. for IMPROVED CRYOSTAT WITH EXTERNAL REFRIGERATOR FOR SUPERCONDUCTING NMR SPECTROMETER Abstract of the Disclosure An improved cryostat for the superconducting magnet of an NMR spectrometer comprises a nested structure of isothermal shells surrounding a thermally conductive central reservoir of substantially spherical shape containing liquid helium in which the superconducting solenoid remains operational when only partially immersed. A radiation shield surrounding the central reservoir is cooled by the boil-off of escaping helium vapor. The radiation shield is enclosed within an isothermal shell maintained at the temperature of liquid nitrogen by thermal contact with a liquid nitrogen reservoir disposed above the region of the central reservoir and shielded therefrom by a wall of the isothermal shell. An outer radiation shield surrounds the liquid nitrogen reservoir and associated isothermal shell and the outer radiation shield is maintained at a temperatures of the order of 235° K by vapor cooling from the boil-off of escaping forms the outer wall of the cryostat sealed containment vessel forms the outer wall of the cryostat and provides all the interior spaces between adjacent nested structures. 2chb21778 -1- 78-08

321935

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