Method and structure for forming a reaction product

B - Operations – Transporting – 01 – J

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23/362, 23/406

B01J 19/00 (2006.01) B01J 3/02 (2006.01) B01J 3/04 (2006.01) B01J 19/18 (2006.01) C01F 11/00 (2006.01) C01G 23/00 (2006.01) C01G 25/00 (2006.01)

Patent

CA 1306098

METHOD AND STRUCTURE FOR FORMING A REACTION PRODUCT Pieter Krijgeman ABSTRACT OF THE DISCLOSURE A reaction product is formed by a process which involves the transfer of the reaction product from an autoclave to a receiving vessel at a substantially constant flow rate. Just prior to this transfer, the pressure in the receiving vessel is brought up to the pressure in the autoclave by passing gas from the autoclave to the receiving vessel. The flow of gas from the autoclave to the receiving vessel is then stopped, and the pressure in the receiving vessel is allowed to drop due to transfer of heat from the gas to the walls of the receiving vessel. The resulting pressure difference between the autoclave and the receiving vessel is used to initiate the transfer of the reaction products from the autoclave to the receiving vessel. A pressure release valve on the receiving vessel is then controlled by means a signal derived from a flow meter which measures the flow rate of the reaction products flowing from the autoclave to the receiving vessel to maintain constant this flow rate.

541073

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