Process for improved sulfure production from sulfure...

C - Chemistry – Metallurgy – 01 – B

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C01B 17/04 (2006.01) B01D 53/48 (2006.01) B01D 53/75 (2006.01)

Patent

CA 2044161

Process for the improvement of the sulphur yield of an assembly which produces sulphur from from H2S and which consists of a sulphur plant (1), an oxidation and hydrolysis unit (2) and a purification unit (3). Said sulphur plant (1) in producing sulphur provides a residual gas (17b) which incorporates H2O, COS and/or CS2 and H2S and SO2 in a mol ratio of H2S:SO2 = 2:1. Said residual gas passes into the unit (2) on a H2S oxidation and COS and CS2 hydrolysis catalyst which functions between 180 C and 700 C, in the presence of air (47), thus producing a residual gas (38) free of COS and CS2 and incorporating H2S and SO2 in a mol ratio which is kept equal to 2:1 by regulating the air flow (47). The residual gas (38) is introduced into the purification unit (3), in which H2S and SO2 are made to react in order to produce sulphur and to obtain a purified residual gas (45).

Procédé pour améliorer le rendement en soufre d'un ensemble produisant du soufre à partir d'H2S et comportant une usine à soufre (1), une unité (2) d'oxydation et d'hydrolyse et une unité (3) d'épuration. L'usine à soufre (1) produit du soufre et fournit un gaz résiduaire (17b), qui renferme H2O, COS et/ou CS2 et H2S et SO2 dans un rapport molaire H2S:SO2 ~ 2:1. Ce gaz résiduaire passe dans l'unité (2) sur un catalyseur d'oxydation de l'H2S et d'hydrolyse de COS et CS2 opérant entre 180°C et 700°C, en présence d'air (47), pour produire un gaz résiduaire (38) exempt de COS et CS2 et renfermant H2S et SO2 dans un rapport molaire maintenu égal à 2:1 par régulation du débit d'air (47). Le gaz résiduaire (38) est introduit dans l'unité (3) d'épuration, dans laquelle on amène H2S et SO2 à réagir pour former du soufre et obtenir un gaz résiduaire épuré (45).

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