A continuous deacetylation and purification process in...

C - Chemistry – Metallurgy – 07 – C

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C07C 231/12 (2006.01) C07C 237/46 (2006.01) C07C 231/22 (2006.01)

Patent

CA 2710594

This invention relates to an improved method for the synthesis of 5-acetamido- N,N'-bis(2,3-dihydroxypropyl)-2,4,6-triiodoisophthalamide ("Compound A"), an intermediate in the industrial preparation of non-ionic X-ray contrast agents. In particular, it relates to a continuous process of deacetylation of the acetylated hydroxyl group in 5-amino- N,N'-bis(2,3-dihydroxypropyl)-2,4,6-triiodo-1,3-benzenedicarboxamide ("Compound B") followed by crystallisations, filtration, and washing of Compound A.

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