Compaction process for manufacture of sodium phenytoin...

A - Human Necessities – 61 – K

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A61K 9/16 (2006.01) A61K 31/4166 (2006.01)

Patent

CA 2446957

A process for the roller compaction and manufacture of a pharmaceutical formulation comprises the steps of adding sodium phenytoin to a vessel of a blender and adding at least one excipient to the vessel. The mixture is blended and transferred to a roller compactor, where pressure is applied to the blend of sodium phenytoin and excipient. Next, the resultant compaction is milled to form a granulation, which is blended a second time and is suitable for further processing into a dosage form. Preferably, the excipients include magnesium stearate, sugar, lactose monohydrate, and talc. In an alternative embodiment, talc is added immediately prior to the granulation being blended for a second time.

L'invention concerne un procédé de compactage et de fabrication à l'aide d'un rouleau de compactage d'une préparation pharmaceutique, consistant à insérer de la phénytoïne de sodium dans un récipient d'un mélangeur et à ajouter au moins un excipient dans le récipient. Le mélange obtenu est mélangé et transféré vers un dispositif muni d'un rouleau de compactage servant à appliquer de la pression sur le mélange de phénytoïne de sodium et d'excipient. Le procédé consiste ensuite à broyer le produit compacté pour former un granulé qui est ensuite mélangé une seconde fois et qui peut être traité ultérieurement pour obtenir une forme posologique. Les excipients utilisés comprennent de préférence du stéarate de magnésium, du sucre, du monohydrate de lactose et du talc. Dans un autre mode de réalisation, le talc est ajouté juste avant que le granulé ne soit mélangé une seconde fois.

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