Method of manufacturing monolithic glass members

C - Chemistry – Metallurgy – 03 – B

Patent

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C03B 19/00 (2006.01) C03B 19/12 (2006.01) C03C 1/00 (2006.01)

Patent

CA 1260712

ABSTRACT: Method of manufacturing monolithic glass members. Monolithic glass members are manufactured by gelating a solution of an alkoxysilane in an alcoholic solvent in an autoclave. In this method, heating is carried out to above the critical temperature of the solvent and when the temperature is reached, the pressure is gradually removed. By providing in the space a pre-pressure of a gas which is so high that upon heating to the desired temperature the overall pressure is always higher than the saturation pressure of the solvent, it is prevented that boiling phenomena can occur.

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