Process and intermediate for the purification of...

Details Process and intermediate for the purification of... Process and intermediate for the purification of...

C - Chemistry, Metallurgy

07

C

C07C 237/26 (2006.01)

Patent

CA 2133198

2133198 9320042 PCTABS00027 The invention relates to a new process for obtaining a completely pure oxytetracycline which does not contain any acetyldecarboxamidooxytetracycline as ingredient. In glacial acetic acid there is suspended under stirring oxytetracycline hydrochloride, or alternatively, oxytetracycline dihydrate under addition of an equimolar quantity of hydrogen chloride in the form of concentrated hydrochloric acid. The stirring is continued for 5 hours, the formed oxytetracycline hydrochloride acetate precipitate is filtered, washed with glacial acetic acid and acetone, whereupon it is dried under reduced pressure at a temperature up to 40 ·C till constant weight. Oxytetracycline hydrochloride acetate of formula (III) is a new compound and may be used as intermediate in the above process.

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