Process for continuous crystallization of alpha mono hydrate...

C - Chemistry – Metallurgy – 13 – B

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260/234.6

C13B 20/16 (2011.01) C07H 3/02 (2006.01) C13K 1/10 (2006.01)

Patent

CA 1175821

3248 ABSTRACT OF THE DISCLOSURE A process for continuously crystallizing alpha mono- hydrate dextrose from dextrose-containing liquours. The process is operated isothermally and produces a lean phase massecuite. According to the process, a rate of agitation is employed, within a reaction zone operated in a continu- ous mode, which permits linear growth of crystals to occur at a growth rate which is surface reaction controlled. The process may be combined with a batch process by feeding lean phase massecuite from the process into a second reaction zone operated in a batch mode. This is done at a constantly declining temperature and produces a rich phase massecuite. The batch process stage is also continuously agitated, but at a slower rate than the first stage continuous process to prevent excessive attrition of existing crystals while maximizing crystal yield.

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