Process for recovering purified, oxidized, renatured...

C - Chemistry – Metallurgy – 07 – K

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530/13, 195/71,

C07K 14/55 (2006.01) C07K 1/113 (2006.01) C07K 1/36 (2006.01) C12N 15/26 (2006.01)

Patent

CA 1337671

A process for recovering highly pure, recombinant IL-2 from transformed microorganisms in which the cells are disrupted; impure recombinant IL-2 is isolated in the form of refractile bodies from the disruptate; the impure IL-2 is dissolved and denatured with at least 6 M guanidine hydrochloride containing a reducing agent; the reduced IL-2 is precipitated and resolubilized; the reduced solubilized IL-2 therein is oxidized by a controlled oxidation in which the con- centration of guanidine hydrochloride is maintained at least at 6 M; the oxidized IL-2 is refolded by reducing the concentration of guanidine hydrochloride in the solution; and the oxidized, refolded IL-2 is further purified by ion exchange chromatography or hydrophobic interaction chromatography and ion exchange chroma- tography.

563757

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