Quantification of the quality of fluidization using a...

C - Chemistry – Metallurgy – 07 – C

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23/370, 260/660.

C07C 17/156 (2006.01) B01J 8/24 (2006.01) B01J 12/00 (2006.01) C07C 19/045 (2006.01)

Patent

CA 1272490

ABSTRACT OF THE DISCLOSURE A fluid-bed reactor is operated in such a way as to better control the desired level of fluidization of the catalyst in the reactor, thereby resulting in a more trouble-free process, the desired level of fluidization is controlled by the use of a thermocouple in the fluid bed which measures temperature fluctuations in the range of from 0.1°F to 0.5 F; this measured temperature is compared to an average temperature and a standard deviation is calculated which quantifies the quality of fluidization; the ratio of reactants entering the fluid-bed reactor are adjusted to maintain the standard deviation below a preselected numerical value; the proclivity to stickiness of the catalyst in the reactor, which is deleterious to the efficiency is thus overcome.

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